ROYALPROBE™AUTOMAS (3.2 mm)
AUTOMAS Probe (1 mm ／ 8 mm)

Features

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This is a high throughput solid-state NMR probe which is a breakthrough for liquid NMR users who have been experiencing difficulty with solid-state NMR measurement. Routine measurements can be performed with the same ease of use as liquid NMR's. The lineup includes the following two types.

• ROYAL Probe^TM AUTOMAS (3.2mm)

• AUTOMAS Probe (1mm, 8mm)

The features of the ROYAL Probe^TMAUTOMAS*/AUTOMAS^§ Probe are:

• Connection and disconnection work is not required during exchange of solid sample ^{※ §}

• The existing auto-tune function can be used ^{※ §}

• The existing Auto Sample Changers can be used ^{※ §}

• Magic angle auto adjustment function ^{※ §}

• Seamless auto-tuning of ³¹P to ¹⁵N nuclei ^※

• Measurements at a wider range of temperatures can be performed ^※

Smooth sample exchange

Probe exchange that was required in solid state NMR measurements becomes unnecessary. By setting a solid sample tube housed in the ROTORCARRIER™ having the same appearance as the rotor used for the liquid sample tubes, samples can be smoothly loaded and ejected from above the magnet via the ROTORCARRIER™ without touching the probe in the same way as using the liquid samples.

Automatic tuning

Unlike liquid NMR probes, the solid probes require manual tuning. The ROYAL Probe™ AUTOMAS/AUTOMAS Probe has the ability to use the same Auto Tuning Unit as the liquid NMR probes, making it possible to tune various nuclei without touching the probe.

Moreover, ROYAL Probe^TM AUTOMAS/AUTOMAS Probe has a built-in slider unit that allows seamless tuning of the nuclei from ³¹P to ¹⁵N, without the need to exchange tuning sticks which have been required with conventional solid-state NMR probes.

Continuous automatic measurements

The ROYAL Probe^TM AUTOMAS/AUTOMAS Probe has the ability to use the existing Auto Sample Changer as is^*1 . Continuous automatic measurements are possible just by setting the ROTORCARRIER^TM loaded with the solid sample tube in a slot of the Auto Sample Changer, and specifying measurement conditions, such as pulse sequences, sample spinning speed, and temperature, on the Delta NMR software in the same fashion as the liquid-state NMR measurements.

Sample is loaded from any slot of auto sample changer.

Automatic adjustment of magic angle

With the ROYAL Probe™ AUTOMAS/AUTOMAS Probe, the NMR software Delta allows for automatic adjustment of a magic angle. Simply insert a sample tube with a standard sample of KBr and click the adjustment start button. A manual adjustment is also possible as required.

ROYAL Probe™ AUTOMAS/AUTOMAS Probe are compatible with the JNM-ECZ, JNM-ECZ Luminous™ series.

• Compatible auto sample changers are ASC24, JackBeam 30, 64, and 100.

Catalogue Download

Automated Solid State NMR System －A solid NMR probe with the throughput of a liquid NMR probe－

Application

Application 3.2mm_AutoMAS_Probe

AUTOMAS：Efficient time management in solid state NMR

AUTOMAS Probe: A solids probe with the throughput of a liquids probe

8 mm AUTOMAS probe

More Info