Quick solid-state NMR measurements by 8 mm MAS:Natural-abundance 43Ca NMR
NM110008E
Great difficulty in 43Ca NMR due to low sensitivity…
- Small gyromagnetic ratio: 40.37 MHz (1H:600MHz)
- Low natural abundance: 0.145 %
- Half-integer quadrupolar nuclei: I = 7/2
8 mm MAS opens a way to natural-abundance 43Ca NMR!

Sample: synthesized tobermorite
Measurements: 43Ca single pulse (in natural abundance)
Spectrometer: JNM-ECA600
Repetition time: 0.5 s
Number of scans: 350,000 scans (ca 2 days)
Measurements: 43Ca single pulse (in natural abundance)
Spectrometer: JNM-ECA600
Repetition time: 0.5 s
Number of scans: 350,000 scans (ca 2 days)
Sample courtesy of
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