Make it possible to measure a small amount of fluorine samples - 19F MAS probe -
NM090007E
19F MAS probe is recommended for the users who want to:
・Observe small 19F signals;
・Reduce spinning sidebands;
・Improve quantitative evaluation,
in 19F solid-state NMR spectroscopy.
Three advantages of 19F MAS probe
#1. Significant reduction of 19F background signals.
Weak signals can be observed.
#2. Fast spinning. (2.5mm: 35kHz, 3.2mm: 24kHz, 4mm: 19kHz)
Spinnning sidebands are greatly reduced.
#3. Strong RF irradiation.
Wide frequency ranges are uniformly excited.
CPMAS vs. 19F MAS probes
19F MAS spectra of a grain of fluorine rubber observed using CPMAS probe (left) and 19F MAS probe (right).
19F background signals
become 1/100.
Effects of fast spinning
19F MAS spectra of PCTFE observed at the spinning frequencies of 24kHz (upper) and 10kHz (lower).
Spinning sidebands
are greatly reduced.
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